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Ch j cxg. A wide range of C–H activation reactions have emerged as promising tools for organic synthesis over the past two decades However, the development of enantioselective C–H activation reactions has met with limited success in terms of efficiency and scope ()Enantioselective carbene insertions into prochiral methylene C–H bonds adjacent to heteroatoms have been achieved in synthetically. O v E F A desknet's(S!. ~ j C x g E l ^ C h E ̖ ͂ɉ Ē ̔\ ͂ ㏸ ܂ B 40 ̏ꍇ A ̑S X e ^ X 3 ㏸ ܂ B.

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We report Ircatalyzed intramolecular silylation of secondary alkyl C–H bonds (Hydrido)silyl ethers, generated in situ by dehydrogenative coupling of a tertiary or conformationally restricted secondary alcohol with diethylsilane, undergo regioselective silylation at a secondary C–H bond γ to the hydroxyl group Oxidation of the resulting oxasilolanes in the same vessel generates 1,3diols. Ucomic B'sLOG v ɂđ D A ڒ ́u N C h v A Җ ̑ 2 6/1 ɔ ܂ I L O āA j i u801 v ɂăR { C x g { !!. R E r ׁE K q b v A b v ʂ T g I r p c ̒ ԃX ^ C y X g b ` p c E u c J b g ^ C v E O ^NO301 F z ł B o A A K A _ X A s A I t B X p c ɑ l C ̔ r p c B p ӂ Ă܂ B.

C h o g J h Q ̃I X X J h ̏Љ y W ł B e Љ A Ǘ l r A S J h ꗗ Ȃ t @ C i ~ b V _ C X Q ƌĂ΂ { Ŗ S Ă̖ K ɂ J h B HP ̂P O O O ͂ ̂́A ɋ ł B ɃC x g J h ̎g p ̂ŁA C ɏ ܂ B. As a consequence, the C−H borylation of (hetero)arenes provides a flexible and reliable platform to realize many indirect aromatic C−H bond functionalization reactions ()By virtue of the relay of aryl boronic ester, many groups have disclosed the conversion from C−H bonds to C−D, C−(hetero)aryl, C−OR, C−NR 2, C−X, C−CN, etcAt the same time, this strategy has been utilized. 265k Followers, 192 Following, 77 Posts See Instagram photos and videos from 천재인 JANE CHUN (@janechun).

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